HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23113983, compound → 7-Amino-2,2,4,5,6-pentamethyl-1-benzofuran-3(2H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23113983 | HCID 23113983 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | 7-Amino-2,2,4,5,6-pentamethyl-1-benzofuran-3(2H)-one | HCID 23114144 | — |
Reaction Steps
Using 7-(benzylamino)-2,2,4,5,6-pentamethyl-1-benzofuran-3(2H)-one obtained in Reference Example 53, the title compound was synthesized in the same manner as in Reference Example 30. Yield: quantitative. Melting point: 141-142° C. (ethyl acetate-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07507841B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-32c37e0b60494dd7b26c55a4580caac5 |
| Source note | uspto-grants-2009_03 |