HCID 86618054, compound → HCID 23113955, compound

HRID 1787137Notes

Reaction equation

HRID 1787137 reaction equation
[CH:1]([C:4]1[CH:25]=[CH:24][C:7]([CH2:8][C:9]2[C:21]([CH3:22])=[CH:20][C:19]([CH3:23])=[CH:18][C:10]=2[O:11][CH2:12][C:13]([O:15]CC)=[O:14])=[CH:6][CH:5]=1)([CH3:3])[CH3:2]>C(OCC)(=O)C.CCCCCC>[CH:1]([C:4]1[CH:5]=[CH:6][C:7]([CH2:8][C:9]2[C:21]([CH3:22])=[CH:20][C:19]([CH3:23])=[CH:18][C:10]=2[O:11][CH2:12][C:13]([OH:15])=[O:14])=[CH:24][CH:25]=1)([CH3:3])[CH3:2]

Participants

3

Reactant 1

HCID 86618054HCID 86618054, compound

Product 1

HCID 23113955HCID 23113955, compoundYield 75%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using ethyl (2-(4-isopropylbenzyl)-3,5-dimethylphenoxy)acetate obtained in Reference Example 154, the title compound was synthesized in the same manner as in Reference Example 156. Yield 75%. Melting point: 104-105° C. (ethyl acetate-hexane).

Workup

  1. customobtained in Reference Example 154

Sources & evidence

ORD record
ord-76f55b6ab6db4b9986f1d9db704a757d
Source dataset
uspto-grants-2009_03
Patent number
US07507841B2

Reaction notes

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