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HRID1787143

反应详情

EQUATION

反应方程式

HRID 1787143 的结构方程式

REACTANTS

反应物

3
结构：Cc1cc(C)c(C)c(O)c1
HCID12769

2,3,5-Trimethylphenol

C9H12O

结构：Cc1cc(O)c(C)c(C)c1Br
HCID3629334

4-bromo-2,3,5-trimethylphenol

C9H11BrO

结构：CC(C)c1ccc(C(=O)CBr)cc1
HCID14042756

2-Bromo-1-[4-(propan-2-yl)phenyl]ethan-1-one

C11H13BrO

PRODUCTS

生成物

1
结构：Cc1cc(OCC(=O)c2ccc(C(C)C)cc2)c(C)c(C)c1Br
HCID23114325

未命名化合物

收率 51%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCCC.CCOC(C)=O
溶剂HCID21226206

未命名化合物

PROCEDURE

实验过程

Using 2,3,5-trimethylphenol, 4-bromo-2,3,5-trimethylphenol was synthesized in the same manner as in Reference Example 23. Using this compound and 2-bromo-1-(4-isopropylphenyl)ethanone obtained in Reference Example 164, the title compound was synthesized in the same manner as in Reference Example 159. Yield 51%. Melting point: 71-72° C. (ethyl acetate-hexane).

WORKUP

后处理

  1. customwas synthesized in the same manner as in Reference Example 23
  2. customobtained in Reference Example 164