HCID 23114022, compound → 6-Methylindan-4-ol

HRID 1787148Notes

Reaction equation

HRID 1787148 reaction equation
C([O:4][C:5]1[CH:13]=[C:12]([CH3:14])[CH:11]=[C:10]2[C:6]=1[CH2:7][CH2:8][CH2:9]2)(=O)C>CCCCCC.C(OCC)(=O)C>[CH3:14][C:12]1[CH:13]=[C:5]([OH:4])[C:6]2[CH2:7][CH2:8][CH2:9][C:10]=2[CH:11]=1

Participants

3

Reactant 1

HCID 23114022HCID 23114022, compound

Product 1

HCID 884746-Methylindan-4-olYield 81%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using 6-methyl-2,3-dihydro-1H-inden-4-yl acetate synthesized in Reference Example 174, the title compound was synthesized in the same manner as in Reference Example 175. Yield 81%. Melting point: 82-83° C. (hexane-ethyl acetate).

Workup

  1. customsynthesized in Reference Example 174

Sources & evidence

ORD record
ord-38527b9b346c41dcbacd909ffc5940c2
Source dataset
uspto-grants-2009_03
Patent number
US07507841B2

Reaction notes

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