2,5-Dimethylphenol → HCID 68709704, compound

HRID 1787170Notes

Reaction equation

HRID 1787170 reaction equation
O[CH:2]([C:6]1[CH:11]=[CH:10][C:9]([CH:12]([CH3:14])[CH3:13])=[CH:8][CH:7]=1)[C:3]([OH:5])=[O:4].[CH3:15][C:16]1[CH:21]=[CH:20][C:19]([CH3:22])=[CH:18][C:17]=1O>CCCCCC.C(OCC)(=O)C>[CH:12]([C:9]1[CH:10]=[CH:11][C:6]([CH:2]2[C:17]3[C:16]([CH3:15])=[CH:21][CH:20]=[C:19]([CH3:22])[C:18]=3[O:5][C:3]2=[O:4])=[CH:7][CH:8]=1)([CH3:14])[CH3:13]

Participants

4

Reactant 2

HCID 72672,5-DimethylphenolHCID 23423233Hydroxy(4-isopropylphenyl)acetic acid

Product 1

HCID 68709704HCID 68709704, compoundYield 20%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using hydroxy(4-isopropylphenyl)acetic acid and 2,5-dimethylphenol synthesized in Reference Example 1, the title compound was synthesized in the same manner as in Reference Example 2. Yield 20%. Melting point: 107-109° C. (hexane-ethyl acetate).

Workup

  1. customsynthesized in Reference Example 1

Sources & evidence

ORD record
ord-cc683a799c084f41bca172646b3cd04b
Source dataset
uspto-grants-2009_03
Patent number
US07507841B2

Reaction notes

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