HCID 68709704, compound → HCID 23114207, compound

HRID 1787172Notes

Reaction equation

HRID 1787172 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([CH:10]2[C:14]3[C:15]([CH3:20])=[CH:16][CH:17]=[C:18]([CH3:19])[C:13]=3[O:12][C:11]2=[O:21])=[CH:6][CH:5]=1)([CH3:3])[CH3:2]>CCCCCC.C(OCC)(=O)C>[OH:21][CH2:11][CH:10]([C:14]1[C:15]([CH3:20])=[CH:16][CH:17]=[C:18]([CH3:19])[C:13]=1[OH:12])[C:7]1[CH:6]=[CH:5][C:4]([CH:1]([CH3:3])[CH3:2])=[CH:9][CH:8]=1

Participants

3

Reactant 1

HCID 68709704HCID 68709704, compound

Product 1

HCID 23114207HCID 23114207, compoundYield 88%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using 3-(4-isopropylphenyl)-4,7-dimethyl-1-benzofuran-2(3H)-one synthesized in Reference Example 230, the title compound was synthesized in the same manner as in Reference Example 8. Yield 88%. Melting point: 88-89° C. (hexane-ethyl acetate).

Workup

  1. customsynthesized in Reference Example 230

Sources & evidence

ORD record
ord-b779b47d889640da96c5e7668cbcfd13
Source dataset
uspto-grants-2009_03
Patent number
US07507841B2

Reaction notes

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