HCID 11694537, compound → HCID 23114098, compound

HRID 1787173Notes

Reaction equation

HRID 1787173 reaction equation
O[CH2:2][CH:3]([C:10]1[C:15]([CH3:16])=[CH:14][C:13]([CH3:17])=[C:12]([CH3:18])[C:11]=1[OH:19])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1>CO>[CH3:16][C:15]1[C:10]2[CH:3]([C:4]3[CH:5]=[CH:6][CH:7]=[CH:8][CH:9]=3)[CH2:2][O:19][C:11]=2[C:12]([CH3:18])=[C:13]([CH3:17])[CH:14]=1

Participants

3

Reactant 1

HCID 11694537HCID 11694537, compound

Product 1

HCID 23114098HCID 23114098, compoundYield 95%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Using 2-(2-hydroxy-1-(phenyl)ethyl)-3,5,6-trimethylphenol obtained in Reference Example 231, the title compound was synthesized in the same manner as in Reference Example 13. Yield 95%. Melting point: 72-73° C. (methanol).

Workup

  1. customobtained in Reference Example 231

Sources & evidence

ORD record
ord-0bbaca243d674e24814d9e921e14c104
Source dataset
uspto-grants-2009_03
Patent number
US07507841B2

Reaction notes

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