Methanol → HCID 23114137, compound

HRID 1787177Notes

Reaction equation

HRID 1787177 reaction equation
Br[C:2]1[CH:7]=[CH:6][C:5]([CH:8]2[C:12]3[C:13]([CH3:19])=[CH:14][C:15]([CH3:18])=[C:16]([CH3:17])[C:11]=3[O:10][CH2:9]2)=[CH:4][CH:3]=1.[CH3:20][OH:21]>>[CH:20]([C:2]1[CH:7]=[CH:6][C:5]([CH:8]2[C:12]3[C:13]([CH3:19])=[CH:14][C:15]([CH3:18])=[C:16]([CH3:17])[C:11]=3[O:10][CH2:9]2)=[CH:4][CH:3]=1)=[O:21]

Participants

3

Reactant 2

HCID 887MethanolHCID 23114254HCID 23114254, compound

Product 1

HCID 23114137HCID 23114137, compoundYield 73%

Procedure

Using 3-(4-bromophenyl)-4,6,7-trimethyl-2,3-dihydro-1-benzofuran obtained in Reference Example 236, the title compound was synthesized in the same manner as in Reference Example 245. Yield 73%. Melting point: 87-88° C. (methanol).

Workup

  1. customobtained in Reference Example 236

Sources & evidence

ORD record
ord-a3e3b849c26f43609d0310194812dc16
Source dataset
uspto-grants-2009_03
Patent number
US07507841B2

Reaction notes

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