HCID 23114003, compound → HCID 23113941, compound

HRID 1787186Notes

Reaction equation

HRID 1787186 reaction equation
C([NH:8][C:9]1[C:14]([CH3:15])=[CH:13][C:12]([O:16][CH3:17])=[C:11]([CH2:18][C:19]2[CH:24]=[CH:23][C:22]([CH:25]([CH3:27])[CH3:26])=[CH:21][CH:20]=2)[C:10]=1[CH3:28])C1C=CC=CC=1>C(OCC)(=O)C.CCCCCC>[CH:25]([C:22]1[CH:23]=[CH:24][C:19]([CH2:18][C:11]2[C:10]([CH3:28])=[C:9]([NH2:8])[C:14]([CH3:15])=[CH:13][C:12]=2[O:16][CH3:17])=[CH:20][CH:21]=1)([CH3:27])[CH3:26]

Participants

3

Reactant 1

HCID 23114003HCID 23114003, compound

Product 1

HCID 23113941HCID 23113941, compoundYield 86%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using N-benzyl-3-(4-isopropylbenzyl)-4-methoxy-2,6-dimethylaniline obtained in Reference Example 267, the title compound was synthesized in the same manner as in Reference Example 30. Yield 86%. Melting point: 91-92° C. (ethyl acetate-hexane).

Workup

  1. customobtained in Reference Example 267

Sources & evidence

ORD record
ord-03335b1f1f874c46a44bae04bf2e5529
Source dataset
uspto-grants-2009_03
Patent number
US07507841B2

Reaction notes

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