HCID 68705431, compound → HCID 68709661, compound

HRID 1787191Notes

Reaction equation

HRID 1787191 reaction equation
C([NH:8][C:9]1[C:10]([CH3:32])=[C:11]([CH3:31])[C:12]2[O:16][CH2:15][CH:14]([C:17]3[CH:22]=[CH:21][C:20]([C:23]4[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=4)=[CH:19][CH:18]=3)[C:13]=2[C:29]=1[CH3:30])C1C=CC=CC=1>CCCCCC>[C:20]1([C:23]2[CH:24]=[CH:25][CH:26]=[CH:27][CH:28]=2)[CH:21]=[CH:22][C:17]([CH:14]2[C:13]3[C:29]([CH3:30])=[C:9]([NH2:8])[C:10]([CH3:32])=[C:11]([CH3:31])[C:12]=3[O:16][CH2:15]2)=[CH:18][CH:19]=1

Participants

3

Reactant 1

HCID 68705431HCID 68705431, compound

Product 1

HCID 68709661HCID 68709661, compoundYield 89%

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

Using N-benzyl-3-(biphenyl-4-yl)-4,6,7-trimethyl-2,3-dihydro-1-benzofuran-5-amine obtained in Reference Example 279, the title compound was synthesized in the same manner as in Reference Example 30. Yield 89%. Melting point: 149-150° C. (hexane).

Workup

  1. customobtained in Reference Example 279

Sources & evidence

ORD record
ord-db6b6d5027a0425e9f381310d46aa1b5
Source dataset
uspto-grants-2009_03
Patent number
US07507841B2

Reaction notes

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