HCID 68708725, compound → HCID 68709068, compound

HRID 1787192Notes

Reaction equation

HRID 1787192 reaction equation
C([NH:8][C:9]1[C:10]([CH3:31])=[C:11]([CH3:30])[C:12]2[O:16][CH2:15][CH:14]([C:17]3[CH:22]=[CH:21][C:20]([CH:23]4[O:27][CH2:26][CH2:25][O:24]4)=[CH:19][CH:18]=3)[C:13]=2[C:28]=1[CH3:29])C1C=CC=CC=1>CCCCCC>[O:24]1[CH2:25][CH2:26][O:27][CH:23]1[C:20]1[CH:19]=[CH:18][C:17]([CH:14]2[C:13]3[C:28]([CH3:29])=[C:9]([NH2:8])[C:10]([CH3:31])=[C:11]([CH3:30])[C:12]=3[O:16][CH2:15]2)=[CH:22][CH:21]=1

Participants

3

Reactant 1

HCID 68708725HCID 68708725, compound

Product 1

HCID 68709068HCID 68709068, compoundYield 87%

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

Using N-benzyl-3-(4-(1,3-dioxolan-2-yl)phenyl)-4,6,7-trimethyl-2,3-dihydro-1-benzofuran-5-amine obtained in Reference Example 284, the title compound was synthesized in the same manner as in Reference Example 30. Yield 87%. Melting point: 125-136° C. (hexane).

Workup

  1. customobtained in Reference Example 284

Sources & evidence

ORD record
ord-2e94f2e99b4a4a5789fb996cddad873a
Source dataset
uspto-grants-2009_03
Patent number
US07507841B2

Reaction notes

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