HCID 68707126, compound → HCID 68709636, compound

HRID 1787193Notes

Reaction equation

HRID 1787193 reaction equation
C([NH:8][C:9]1[C:10]([CH3:28])=[C:11]([CH3:27])[C:12]2[O:16][CH:15]=[C:14]([C:17]3[CH:22]=[CH:21][C:20]([CH2:23][CH3:24])=[CH:19][CH:18]=3)[C:13]=2[C:25]=1[CH3:26])C1C=CC=CC=1>C(OCC)(=O)C.CCCCCC>[CH2:23]([C:20]1[CH:21]=[CH:22][C:17]([C:14]2[C:13]3[C:25]([CH3:26])=[C:9]([NH2:8])[C:10]([CH3:28])=[C:11]([CH3:27])[C:12]=3[O:16][CH:15]=2)=[CH:18][CH:19]=1)[CH3:24]

Participants

3

Reactant 1

HCID 68707126HCID 68707126, compound

Product 1

HCID 68709636HCID 68709636, compoundYield 85%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using N-benzyl-3-(4-ethylphenyl)-4,6,7-trimethyl-1-benzofuran-5-amine obtained in Reference Example 281, the title compound was synthesized in the same manner as in Reference Example 30. Yield 85%. Melting point: 68-69° C. (ethyl acetate-hexane).

Workup

  1. customobtained in Reference Example 281

Sources & evidence

ORD record
ord-a7a51242f7d540918c1ea97fa072f57d
Source dataset
uspto-grants-2009_03
Patent number
US07507841B2

Reaction notes

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