HCID 68710597, compound → HCID 23114212, compound

HRID 1787215Notes

Reaction equation

HRID 1787215 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2([CH3:22])[C:14]3[CH:15]=[C:16]([NH2:21])[C:17]([CH3:20])=[C:18]([CH3:19])[C:13]=3[O:12][CH2:11]2)=[CH:6][CH:5]=1)([CH3:3])[CH3:2]>C(OCC)(=O)C.CCCCCC>[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2([CH3:22])[C:14]3[CH:15]=[C:16]([NH:21][C:13](=[O:12])[CH2:14][C:10]([CH3:22])([CH3:11])[CH3:7])[C:17]([CH3:20])=[C:18]([CH3:19])[C:13]=3[O:12][CH2:11]2)=[CH:6][CH:5]=1)([CH3:3])[CH3:2]

Participants

3

Reactant 1

HCID 68710597HCID 68710597, compound

Product 1

HCID 23114212HCID 23114212, compoundYield 59%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using 3-(4-isopropylphenyl)-3,6,7-trimethyl-2,3-dihydro-1-benzofuran-5-amine obtained in Reference Example 35, the title compound was synthesized in the same manner as in Example 1. Yield: 59%. Melting point: 132-133° C. (ethyl acetate-hexane).

Workup

  1. customobtained in Reference Example 35

Sources & evidence

ORD record
ord-d20509fd09234d88852c8a636e8a4faa
Source dataset
uspto-grants-2009_03
Patent number
US07507841B2

Reaction notes

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