Ethyl acetate hexane → HCID 86612353, compound

HRID 1787244Notes

Reaction equation

HRID 1787244 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([CH:10]2[C:14]3[C:15]([CH3:23])=[C:16]([NH:20][CH:21]=[O:22])[C:17]([CH3:19])=[CH:18][C:13]=3[O:12][CH2:11]2)=[CH:6][CH:5]=1)([CH3:3])[CH3:2].CCCCCC.[C:30](OCC)(=[O:32])C>>[CH:30]([C:18]1[C:13]2[O:12][CH2:11][CH:10]([C:7]3[CH:6]=[CH:5][C:4]([CH:1]([CH3:3])[CH3:2])=[CH:9][CH:8]=3)[C:14]=2[C:15]([CH3:23])=[C:16]([NH:20][CH:21]=[O:22])[C:17]=1[CH3:19])=[O:32]

Participants

3

Reactant 2

HCID 21226206Ethyl acetate hexaneHCID 23114243HCID 23114243, compound

Product 1

HCID 86612353HCID 86612353, compoundYield 92%

Procedure

Using (3-(4-isopropylphenyl)-4,6-dimethyl-2,3-dihydro-1-benzofuran-5-yl)formamide obtained in Example 58, the title compound was synthesized in the same manner as in Example 20. Yield: 92%. Melting point: 123-124° C. (hexane-ethyl acetate).

Sources & evidence

ORD record
ord-41bb6c0ccf86424caf87f07adfde958c
Source dataset
uspto-grants-2009_03
Patent number
US07507841B2

Reaction notes

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