HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23113986, compound → HCID 23114280, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23113986 | HCID 23113986 | — |
| Reactant | HCID 178418443 | HCID 178418443 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 23114280 | HCID 23114280 | 22% |
Reaction Steps
Using N-(7-formyl-3-(4-isopropylphenyl)-4,6-dimethyl-2,3-dihydro-1-benzothien-5-yl)-3,3-dimethylbutanamide obtained in Example 163 and ethylmagnesium bromide, the title compound was synthesized in the same manner as in Example 164. Yield: 22%. Melting point: 159-160° C. (hexane-ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07507841B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-58d1bf4d2c224d13bc8d41580bfbde7a |
| Source note | uspto-grants-2009_03 |