Cyclohexylamine → HCID 23114383, compound

HRID 1787334Notes

Reaction equation

HRID 1787334 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([CH:10]2[C:14]3[C:15]([CH3:30])=[C:16]([NH:21][C:22](=O)[O:23]CC(Cl)(Cl)Cl)[C:17]([CH3:20])=[C:18]([CH3:19])[C:13]=3[O:12][CH2:11]2)=[CH:6][CH:5]=1)([CH3:3])[CH3:2].[CH:31]1([NH2:37])[CH2:36][CH2:35][CH2:34][CH2:33][CH2:32]1>>[CH:31]1([NH:37][C:22]([NH:21][C:16]2[C:17]([CH3:20])=[C:18]([CH3:19])[C:13]3[O:12][CH2:11][CH:10]([C:7]4[CH:6]=[CH:5][C:4]([CH:1]([CH3:3])[CH3:2])=[CH:9][CH:8]=4)[C:14]=3[C:15]=2[CH3:30])=[O:23])[CH2:36][CH2:35][CH2:34][CH2:33][CH2:32]1

Participants

3

Reactant 2

HCID 7965CyclohexylamineHCID 86618058HCID 86618058, compound

Product 1

HCID 23114383HCID 23114383, compoundYield 92%

Procedure

Using 2,2,2,-trichloroethyl (3-(4-isopropylphenyl)-4,6,7-trimethyl-2,3-dihydro-1-benzofuran-5-yl)carbamate obtained in Example 138 and cyclohexylamine, the title compound was obtained in the same manner as in Example 143.

Sources & evidence

ORD record
ord-af1990caf7b34e9b9fec885fd104bfbd
Source dataset
uspto-grants-2009_03
Patent number
US07507841B2

Reaction notes

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