huagongshe.com
HRID1787343

反应详情

EQUATION

反应方程式

HRID 1787343 的结构方程式

REACTANTS

反应物

1
结构：Cc1c(NC(=O)CC(C)(C)C)cc2c(c1C)OC(C)(C)C2=O
HCID23113858

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c(NC(=O)CC(C)(C)C)cc2c(c1C)OC(C)(C)C2O
HCID23114263

未命名化合物

收率 92%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1.CCCCCC
溶剂HCID21883165

未命名化合物

PROCEDURE

实验过程

Using 3,3-dimethyl-N-(2,2,6,7-tetramethyl-3-oxo-2,3-dihydro-1-benzofuran-5-yl)butanamide obtained in Reference Example 65, the title compound was synthesized in the same manner as in Example 234. Yield: 92%. Melting point: 184-185° C. (THF-hexane).

WORKUP

后处理

  1. customobtained in Reference Example 65