HCID 23114146, compound → HCID 23114317, compound

HRID 1787357Notes

Reaction equation

HRID 1787357 reaction equation
[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]1(O)[C:10]2[CH:11]=[C:12]([NH:17][C:18](=[O:24])[CH2:19][C:20]([CH3:23])([CH3:22])[CH3:21])[C:13]([CH3:16])=[C:14]([CH3:15])[C:9]=2[O:8][C:7]1([CH3:26])[CH3:25]>C(OCC)(=O)C.CCCCCC>[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]1[C:10]2[CH:11]=[C:12]([NH:17][C:18](=[O:24])[CH2:19][C:20]([CH3:22])([CH3:21])[CH3:23])[C:13]([CH3:16])=[C:14]([CH3:15])[C:9]=2[O:8][C:7]1([CH3:26])[CH3:25]

Participants

3

Reactant 1

HCID 23114146HCID 23114146, compound

Product 1

HCID 23114317HCID 23114317, compoundYield 67%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

Using N-(3-(2-furyl)-3-hydroxy-2,2,6,7-tetramethyl-2,3-dihydro-1-benzofuran-5-yl)-3,3-dimethylbutanamide obtained in Example 252, the title compound was synthesized in the same manner as in Example 271. Yield: 67%. Melting point: 126-127° C. (ethyl acetate-hexane).

Sources & evidence

ORD record
ord-231df57612eb464f9b642537ecdceb90
Source dataset
uspto-grants-2009_03
Patent number
US07507841B2

Reaction notes

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