huagongshe.com
HRID1787358

反应详情

EQUATION

反应方程式

HRID 1787358 的结构方程式

REACTANTS

反应物

1
结构：Cc1c(NC(=O)CC(C)(C)C)cc2c(c1C)OC(C)(C)C2(O)CCc1ccccc1
HCID23113920

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c(NC(=O)CC(C)(C)C)cc2c(c1C)OC(C)(C)C2CCc1ccccc1
HCID23114281

未命名化合物

收率 92%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCCC.CCOC(C)=O
溶剂HCID21226206

未命名化合物

PROCEDURE

实验过程

Using N-(3-hydroxy-2,2,6,7-tetramethyl-3-(2-phenylethyl)-2,3-dihydro-1-benzofuran-5-yl)-3,3-dimethylbutanamide obtained in Example 240, the title compound was synthesized in the same manner as in Example 271. Yield: 92%. Melting point: 158-159° C. (ethyl acetate-hexane).