HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23114100, compound → HCID 68709094, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23114100 | HCID 23114100 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 68709094 | HCID 68709094 | 74% |
Reaction Steps
Using N-(7-(1-hydroxy(phenyl)methyl)-2,2,4,6-tetramethyl-2,3-dihydro-1-benzofuran-5-yl)-3,3-dimethylbutanamide obtained in Example 355, the title compound was synthesized in the same manner as in Example 271. Yield: 74%. Melting point: 129-130° C. (ethyl acetate-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07507841B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-5a98f2d1812c46c6b79416641375d74c |
| Source note | uspto-grants-2009_03 |