HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 25052164, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 67363743 | HCID 67363743 | — |
| Product | HCID 25052164 | HCID 25052164 | — |
Reaction Steps
) The title compound was prepared from the above described 3′-[8-(isobutyl-methyl-amino)-4-oxo-7-trifluoromethyl-4,5-dihydro-3H-benzo[b][1,4]diazepin-2-yl]-biphenyl-4-sulfonic acid tert-butylamide (250 mg) and TFA (5 mL) according to the general procedure I step 2. Obtained as a white solid (107 mg, 39%). MS (ISN) 543.5 [(M−H)−]; mp 236° C. (dec).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07511033B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-fa2176ad90f842f192b095316d88e53e |
| Source note | uspto-grants-2009_03 |