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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1787442Generated: October 31, 2026

Trifluoroacetic acid → HCID 25049862, compound

https://huagongshe.com/reaction/1787442

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 67362223HCID 67362223—
ProductHCID 25049862HCID 25049862—

Reaction Steps

) The title compound was prepared from the above described 3′-(8-isobutylamino-4-oxo-7-trifluoromethyl-4,5-dihydro-3H-benzo[b][1,4]diazepin-2-yl)-biphenyl-3-sulfonic acid tert-butylamide (275 mg) and TFA (6 mL) according to the general procedure I step 2. Obtained as a yellow solid (172 mg, 65%). MS (ISN) 529.4 [(M−H)−]; mp 251° C. (dec).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07511033B2
Source datasetuspto-grants-2009_03
ORD IDord-1385443903594c5488f9bd8f3b60430d
Source noteuspto-grants-2009_03