4-Nitrophenylboronic acid → HCID 5276055, compound

HRID 1788456Notes

Reaction equation

HRID 1788456 reaction equation
[CH:1]1([N:7]2[C:11]3[CH:12]=[CH:13][C:14]([C:16]([OH:18])=[O:17])=[CH:15][C:10]=3[N:9]=[C:8]2[C:19]2[CH:20]=[C:21]3[C:26](=[CH:27][CH:28]=2)[N:25]=[C:24]([C:29]2[C:34](C4C=CC(OC)=C(OC)C=4)=[CH:33][CH:32]=[C:31]([C:45]([N:47]4[CH2:51][CH2:50][CH2:49][CH2:48]4)=[O:46])[CH:30]=2)[CH:23]=[CH:22]3)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[N+:52]([C:55]1[CH:60]=[CH:59][C:58](B(O)O)=[CH:57][CH:56]=1)([O-:54])=[O:53]>>[CH:1]1([N:7]2[C:11]3[CH:12]=[CH:13][C:14]([C:16]([OH:18])=[O:17])=[CH:15][C:10]=3[N:9]=[C:8]2[C:19]2[CH:20]=[C:21]3[C:26](=[CH:27][CH:28]=2)[N:25]=[C:24]([C:29]2[C:34]([C:58]4[CH:59]=[CH:60][C:55]([N+:52]([O-:54])=[O:53])=[CH:56][CH:57]=4)=[CH:33][CH:32]=[C:31]([C:45]([N:47]4[CH2:51][CH2:50][CH2:49][CH2:48]4)=[O:46])[CH:30]=2)[CH:23]=[CH:22]3)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 27735524-Nitrophenylboronic acidHCID 5276039HCID 5276039, compound

Product 1

HCID 5276055HCID 5276055, compound

Procedure

The title compound (5.2 mg yield) was prepared as described for Compound 419 using 4-nitrophenylboronic acid in place of 3,4-dimethoxyphenylboronic acid.

Sources & evidence

ORD record
ord-a95e450f826d44a79035dcf9ee69447b
Source dataset
uspto-grants-2009_03
Patent number
US07511145B2

Reaction notes

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