HRID1788470

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID2733954

6-Amino-2-naphthoic acid

C11H9NO2

结构：O=C(NN1CCOCC1)c1ccc2c(c1)nc(-c1ccc3nc(-c4ccccc4)cnc3c1)n2C1CCCCC1

HCID57603045

未命名化合物

PRODUCTS

生成物

结构：O=C(O)c1ccc2cc(NC(=O)c3ccc4c(c3)nc(-c3ccc5nc(-c6ccccc6)cnc5c3)n4C3CCCCC3)ccc2c1

HCID5276176

未命名化合物

收率 53%

PROCEDURE

实验过程

The general procedure described for Compound 574 was used with 6-amino-naphthalene-2-carboxylic acid (18.7 mg), producing 15 mg of the title compound (53% yield). MS: 618.30 (M+H+) HPLC Procedure A, retention time=16.24 min.

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-f90156ac52c440d7a7ecf69af9d377f2
来源数据集: uspto-grants-2009_03
DOI: 10.6084/m9.figshare.5104873.v1
专利: US07511145B2
来源说明: uspto-grants-2009_03

反应 SMILES

N1(N[C:8]([C:10]2[CH:40]=[CH:39][C:13]3[N:14]([CH:33]4[CH2:38][CH2:37][CH2:36][CH2:35][CH2:34]4)[C:15]([C:17]4[CH:18]=[C:19]5[C:24](=[CH:25][CH:26]=4)[N:23]=[C:22]([C:27]4[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=4)[CH:21]=[N:20]5)=[N:16][C:12]=3[CH:11]=2)=[O:9])CCOCC1.[NH2:41][C:42]1[CH:43]=[C:44]2[C:49](=[CH:50][CH:51]=1)[CH:48]=[C:47]([C:52]([OH:54])=[O:53])[CH:46]=[CH:45]2>>[CH:33]1([N:14]2[C:13]3[CH:39]=[CH:40][C:10]([C:8]([NH:41][C:42]4[CH:43]=[C:44]5[C:49](=[CH:50][CH:51]=4)[CH:48]=[C:47]([C:52]([OH:54])=[O:53])[CH:46]=[CH:45]5)=[O:9])=[CH:11][C:12]=3[N:16]=[C:15]2[C:17]2[CH:18]=[C:19]3[C:24](=[CH:25][CH:26]=2)[N:23]=[C:22]([C:27]2[CH:28]=[CH:29][CH:30]=[CH:31][CH:32]=2)[CH:21]=[N:20]3)[CH2:38][CH2:37][CH2:36][CH2:35][CH2:34]1