Nitric Acid → HCID 178524776, compound

HRID 1788547Notes

Reaction equation

HRID 1788547 reaction equation
[OH:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][N:3]=1.[N+:11]([O-])([OH:13])=[O:12]>>[OH:1][C:2]1[C:10]([N+:11]([O-:13])=[O:12])=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][N:3]=1

Participants

3

Reactant 2

HCID 944Nitric AcidHCID 178418479HCID 178418479, compound

Product 1

HCID 178524776HCID 178524776, compound

Procedure

A solution of 6-hydroxynicotinic acid (10 g, 71.89 mmol) in fuming nitric acid (100 mL) was stirred at 50° C. for 4 h. After evaporation of extra nitric acid, the solid was obtained and it was directly used in the next step reaction. MS: 185.02 (M+H+).

Workup

  1. customAfter evaporation of extra nitric acid
  2. customthe solid was obtained
  3. customit was directly used in the next step reaction

Sources & evidence

ORD record
ord-f2bc132c6e9a4ccaa92b2c3e67d2293f
Source dataset
uspto-grants-2009_03
Patent number
US07511145B2

Reaction notes

Loading…