HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 13336368, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | N-Methyl-2-butanamine | HCID 111026 | — |
| Reactant | 3-phenylnaphthalene-1-carboxylic Acid | HCID 10562505 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 13336368 | HCID 13336368 | — |
Reaction Steps
The procedure of Example 20 is followed using 3-phenylnaphthalene-1-carboxylic acid (4.3 g), thionyl chloride (20 ml) and N-methylbut-2-ylamine (1.5 g) in pyridine (20 ml) as the starting materials. After recrystallisation from petroleum ether, N-methyl-N-(1-methylpropyl)-3-phenylnaphthalene-1-carboxamide (2.8 g), melting at 125° C., is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04684652 |
| Source dataset | uspto-grants-1987_08 |
| ORD ID | ord-ca34bcb87e9e457fb9f9bea9ba147c0f |
| Source note | uspto-grants-1987_08 |