Sodium Bicarbonate → HCID 23708850, compound

Participants

Reaction Steps

A mixture of a solution of 56 mg of 4-nitrobenzyl-7-oxo-3-phenoxy-4-thia-1-azabicyclo[3,2,0]hept-2-ene-2-carboxylate in 3 ml of dioxan and 12.5 mg of sodium bicarbonate in 2 ml of water, and 10% palladium/charcoal was hydrogenated at 50 psi at 25° for 90 minutes. The mixture was then filtered through Celite, and lyophilized to yield 30 mg of the title compound as a pale yellow crystalline solid.

Provenance & Evidence