HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyethanol → HCID 20189375, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyethanol | HCID 8019 | — |
| Reactant | Ethyl 4-fluoro-3-oxobutanoate | HCID 9744 | — |
| Product | HCID 20189375 | HCID 20189375 | — |
Reaction Steps
Ethyl 4-fluoro-3-oxobutanoate (2.1 g) was heated at reflux in 2-methoxyethanol (10 ml) for 3 hours. The solvent was removed in vacuo and the residue distilled to give the title compound as a colourless oil (1.75 g). Nmr (CDCl3)δ4.9 (d,2H,J-48 Hz), 3.4 (s,3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04686217 |
| Source dataset | uspto-grants-1987_08 |
| ORD ID | ord-703dd6a1b43d49a5ba396824236d92dc |
| Source note | uspto-grants-1987_08 |