Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methacrylic Acid | HCID 4093 | — |
| Reactant | Allyl methacrylate | HCID 7274 | — |
| Reactant | 2,2'-Azobis(2,4-dimethylvaleronitrile) | HCID 91537 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 86588650 | HCID 86588650 | — |
Reaction Steps
The poly(allyl methacrylate/methacrylic acid) was synthesized by the following process. In a 3 l four-necked flask equipped with a stirring bar and a stirring blade, a reflux condenser, a dropping funnel and a thermometer, 1.68 l of 1,2-dichloroethane was placed as a reaction solvent and heated to 70° C. in a nitrogen atmosphere. A solution prepared by dissolving 100.8 g of allyl methacrylate 7.6 g of methacrylic acid and 1.68 g of the polymerization initiator: 2,2'-azobis(2,4-dimethylvaleronitrile) in 0.44 l of 1,2-dichloroethane was placed in a dropping funnel and the mixed solution was added dropwise to the flask with stirring for over 2 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04687727 |
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| Source dataset | uspto-grants-1987_08 |
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| ORD ID | ord-1ef2a53333f948fbaba0c8b3aaad3e06 |
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| Source note | uspto-grants-1987_08 |
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