Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Beta-Alanine | HCID 239 | — |
| Reactant | Phthalic Anhydride | HCID 6811 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3-Phthalimidopropionic acid | HCID 76859 | — |
Reaction Steps
A mixture of phthalic anhydride (500 g) and β-alanine (267 g) was fused by heating at 200° C. for 15 minutes, and poured into water (1500 ml). The formed precipitate was collected by filtration, and recrystallized from ethanol to give phthaloyl-β-alanine (hereinafter referred to as pht-βAla), yield 537 g, 81.6%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04687817 |
|---|
| Source dataset | uspto-grants-1987_08 |
|---|
| ORD ID | ord-e332db8ef9054b4da65d31751cd05d4e |
|---|
| Source note | uspto-grants-1987_08 |
|---|
