Allyltrimethylsilane → Diphenyl[3-(trimethylsilyl)propyl]phosphane

Participants

Reaction Steps

A mixture of 22.8 g (0.2 mole) allyl trimethyl silane and 37.2 g (0.2 mole) diphenyl phosphine was reacted for 158 hours in the manner described in Example 1. A subsequent fractional distillation, yielded the desired pure adduct as a clear, colorless liquid. The distillation yield was 50%. The product had a boiling point of 150° C. at 0.10 mm.

Provenance & Evidence