Thionyl Chloride → HCID 54004179, compound

HRID 1789394Notes

Reaction equation

HRID 1789394 reaction equation
[CH3:1][C:2]1[C:10]2[C:5](=[CH:6][CH:7]=[C:8]([CH3:11])[CH:9]=2)[CH2:4][C:3]=1[C:12]([OH:14])=O.S(Cl)([Cl:17])=O>>[CH3:1][C:2]1[C:10]2[C:5](=[CH:6][CH:7]=[C:8]([CH3:11])[CH:9]=2)[CH2:4][C:3]=1[C:12]([Cl:17])=[O:14]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 13649405HCID 13649405, compound

Product 1

HCID 54004179HCID 54004179, compound

Procedure

3,5-Dimethyl-indene-2-carboxylic acid (37.3 g) is converted to its acid chloride by treatment with thionyl chloride (580 ml). Excess thionyl chloride is distilled off. Yield 40.5 g, 99%.

Workup

  1. distillationExcess thionyl chloride is distilled off

Sources & evidence

ORD record
ord-87df338463cf4ff9b0aae301b7d4b2ce
Source dataset
uspto-grants-1987_08
Patent number
US04689339

Reaction notes

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