Thionyl Chloride → HCID 54550579, compound

HRID 1789403Notes

Reaction equation

HRID 1789403 reaction equation
[CH2:1]([C:3]1([C:13]([OH:15])=O)[CH2:12][CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4]1)[CH3:2].S(Cl)([Cl:18])=O>>[CH2:1]([C:3]1([C:13]([Cl:18])=[O:15])[CH2:12][CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4]1)[CH3:2]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 20188226HCID 20188226, compound

Product 1

HCID 54550579HCID 54550579, compound

Procedure

A mixture of 2-ethyl-1,2,3,4-tetrahydro-2-naphthoic acid (22,0 g) and thionyl chloride is boiled for 5 days. The acid chloride is distilled. B.p. 110°-115° C./0.2 mmHg. Yield 21.6 g, 90%.

Workup

  1. distillationThe acid chloride is distilled

Sources & evidence

ORD record
ord-107362592a79411db3a3bb2ea321f094
Source dataset
uspto-grants-1987_08
Patent number
US04689339

Reaction notes

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