Bromine → HCID 20188229, compound

HRID 1789405Notes

Reaction equation

HRID 1789405 reaction equation
[CH2:1]([C:3]1([C:13](=[O:15])[CH3:14])[CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]1[CH3:12])[CH3:2].[Br:16]Br>C(Cl)Cl>[Br:16][CH2:14][C:13]([C:3]1([CH2:1][CH3:2])[CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]1[CH3:12])=[O:15]

Participants

4

Reactant 2

HCID 24408BromineHCID 20188234HCID 20188234, compound

Product 1

HCID 20188229HCID 20188229, compoundYield 65%

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

2-Bromo-1-(2,3-dihydro-2-ethyl-1-methyl-1H-inden-2-yl)ethanone is prepared from 1-(2,3-dihydro-2-ethyl-1-methyl-1H-inden-2-yl)ethanone (21.6 g) by treatment with bromine (17.6 g) in methylene chloride (300 ml). Yield 65%.

Sources & evidence

ORD record
ord-9d4ebd8e481047809b51612b904aa6b8
Source dataset
uspto-grants-1987_08
Patent number
US04689339

Reaction notes

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