4-Chlorobenzylamine → HCID 13958340, compound

HRID 1789425Notes

Reaction equation

HRID 1789425 reaction equation
Cl[C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[N:5]=[CH:4][C:3]=1[N+:12]([O-:14])=[O:13].[Cl:15][C:16]1[CH:23]=[CH:22][C:19]([CH2:20][NH2:21])=[CH:18][CH:17]=1>>[Cl:15][C:16]1[CH:23]=[CH:22][C:19]([CH2:20][NH:21][C:2]2[C:11]3[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=3)[N:5]=[CH:4][C:3]=2[N+:12]([O-:14])=[O:13])=[CH:18][CH:17]=1

Participants

3

Reactant 2

HCID 660364-ChlorobenzylamineHCID 112758084-Chloro-3-nitroquinoline

Product 1

HCID 13958340HCID 13958340, compound

Procedure

Using the method of Example 1, 4-chloro-3-nitroquinoline was reacted with 4-chlorobenzylamine to provide yellow solid 4-(4-chlorobenzylamino)-3-nitroquinoline, the melting point of the crude product being 168°-173° C.

Sources & evidence

ORD record
ord-70af8be2728549008f36c1cf9792bfa8
Source dataset
uspto-grants-1987_08
Patent number
US04689338

Reaction notes

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