HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminophenol → HCID 14049036, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminophenol | HCID 5801 | — |
| Reactant | HCID 11126439 | HCID 11126439 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 14049036 | HCID 14049036 | — |
Reaction Steps
A mixture of 15 parts of 4-(isothiocyanatomethyl)pyridine, 9.5 parts of 2-aminophenol and 160 parts of acetonitrile was stirred for 3 hours at room temperature. The precipitated product was filtered off, washed with 2,2'-oxybispropane and crystallized from acetonitrile, yielding 8.22 parts of N-(2-hydroxyphenyl)-N'-(4-pyridinylmethyl)thiourea; mp. 179.6° C. (intermediate 73).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04689330 |
| Source dataset | uspto-grants-1987_08 |
| ORD ID | ord-75690f0a653d4186828de4ecee7463a7 |
| Source note | uspto-grants-1987_08 |