Hydrofluoric Acid → HCID 15053054, compound

Participants

Reaction Steps

The procedure followed is the same as that described in Example 23 substituting 3-(5-[(1,1-dimethylethyl)dimethylsiloxyl]but-1-yl)cyclopentene {[4-(2-cyclopenten-1-yl)butoxy](1,1-dimethylethyl)dimethylsilane} (100 g, 0.407 moles), 5% hydrofluoric acid (78 ml), and acetonitrile (1500 ml). The crude product is kugelrohred under reduced pressure leaving a clear, colorless oil (51 g, 0.36 moles).

Provenance & Evidence