HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrofluoric Acid → HCID 15053054, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrofluoric Acid | HCID 14917 | — |
| Reactant | HCID 13924077 | HCID 13924077 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 15053054 | HCID 15053054 | — |
Reaction Steps
The procedure followed is the same as that described in Example 12 substituting 3-(5-[(1,1-dimethylethyl)dimethylsiloxy]but-1-yl)cyclopentene {[4-(2-cyclopenten-1-yl)butoxy](1,1dimethylethyl)dimethylsilane} (100 g, 0.407 moles), 5% hydrofluoric acid (78 ml), acetonitrile (1500 ml). The crude product is kugelrohred under reduced pressure leaving a clear, colorless oil (51 g, 0.36 moles).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04689345 |
| Source dataset | uspto-grants-1987_08 |
| ORD ID | ord-d698bcc6c8a84c5db225fe974c31b177 |
| Source note | uspto-grants-1987_08 |