HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene carbonate → HCID 22036448, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene carbonate | HCID 7303 | — |
| Reactant | 3-Hydroxyacetanilide | HCID 12124 | — |
| Product | HCID 22036448 | HCID 22036448 | 99% |
Reaction Steps
The title product was prepared according to the procedure described in Example 114, Step 1, starting from 3-acetamidophenol (2.10 g, 13.9 mmol) and ethylene carbonate (0.88 g, 10 mmol). The crude product was purified by column chromatography on silica using toluene/EtOAc/MeOH (49:49:2). Oil; yield 99%. MS m/z 195 (M)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07071180B2 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-8e121cbe1c3844068436c6287637441a |
| Source note | uspto-grants-2006_07 |