HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 22041482, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 22041505 | HCID 22041505 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22041482 | HCID 22041482 | — |
Reaction Steps
4 g of the compound obtained in Step C of Example 10 are dissolved in 200 ml of dichloromethane and the temperature is lowered to 0° C. 12.47 ml of trifluoroacetic acid are then added and the reaction mixture is stirred at ambient temperature for 4 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07071221B2 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-b9097aceecf54623a7ba7ac7d11124e7 |
| Source note | uspto-grants-2006_07 |