HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 22041560, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Butyryl chloride | HCID 8855 | — |
| Reactant | HCID 22041482 | HCID 22041482 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22041560 | HCID 22041560 | — |
Reaction Steps
500 mg of the compound obtained in Step A of Example 12 are dissolved in 10 ml of ethyl acetate; 0.353 ml of triethylamine is then added and the temperature is lowered to 0° C. 0.177 ml of butyryl chloride is added and the mixture is allowed to return to ambient temperature and is stirred overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07071221B2 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-5d99a487dd824cc1886a6c201ec4a455 |
| Source note | uspto-grants-2006_07 |