HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetyl chloride → HCID 22041589, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetyl chloride | HCID 7679 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 22041482 | HCID 22041482 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22041589 | HCID 22041589 | — |
Reaction Steps
500 mg of the compound obtained in Step A of Example 12 are dissolved in 10 ml of ethyl acetate; 0.353 ml of triethylamine is then added and the temperature is lowered to 0° C. 0.226 ml of phenylacetyl chloride is added and the mixture is allowed to return to ambient temperature and is stirred overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07071221B2 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-ffab1b33acd54a0e919e87ad681cd354 |
| Source note | uspto-grants-2006_07 |