O-Methylhydroxylamine → HCID 86760133, compound

HRID 1790262Notes

Reaction equation

HRID 1790262 reaction equation
[C:1]([C:9]1[CH:41]=[CH:40][C:12]2[N:13]([CH2:17][CH2:18][O:19][C:20]3[CH:39]=[CH:38][C:23]([CH2:24][CH:25]([CH2:30][CH2:31][C:32]4[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=4)[C:26]([O:28][CH3:29])=[O:27])=[CH:22][CH:21]=3)[C:14](=[O:16])[S:15][C:11]=2[CH:10]=1)(=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:42][O:43][NH2:44]>>[CH3:42][O:43][N:44]=[C:1]([C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1)[C:9]1[CH:41]=[CH:40][C:12]2[N:13]([CH2:17][CH2:18][O:19][C:20]3[CH:39]=[CH:38][C:23]([CH2:24][CH:25]([CH2:30][CH2:31][C:32]4[CH:33]=[CH:34][CH:35]=[CH:36][CH:37]=4)[C:26]([O:28][CH3:29])=[O:27])=[CH:22][CH:21]=3)[C:14](=[O:16])[S:15][C:11]=2[CH:10]=1

Participants

3

Reactant 2

HCID 4113O-MethylhydroxylamineHCID 22041600HCID 22041600, compound

Product 1

HCID 86760133HCID 86760133, compound

Procedure

Starting from the compound obtained in Step A, the procedure is as in Step B of Example 2, replacing the hydroxylamine by O-methylhydroxylamine. The two (Z) and (E) compounds are not separated.

Workup

  1. customThe two (Z) and (E) compounds are not separated

Sources & evidence

ORD record
ord-b3e19273d94248e8a46697073c36fcfe
Source dataset
uspto-grants-2006_07
Patent number
US07071221B2

Reaction notes

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