O-Methylhydroxylamine → HCID 86760137, compound

HRID 1790274Notes

Reaction equation

HRID 1790274 reaction equation
[C:1]([C:4]1[CH:31]=[CH:30][C:7]2[N:8]([CH2:12][CH2:13][O:14][C:15]3[CH:29]=[CH:28][C:18]([O:19][C:20]([CH3:27])([CH3:26])[C:21]([O:23][CH2:24][CH3:25])=[O:22])=[CH:17][CH:16]=3)[C:9](=[O:11])[S:10][C:6]=2[CH:5]=1)(=O)[CH3:2].[CH3:32][O:33][NH2:34]>>[CH3:32][O:33][N:34]=[C:1]([C:4]1[CH:31]=[CH:30][C:7]2[N:8]([CH2:12][CH2:13][O:14][C:15]3[CH:29]=[CH:28][C:18]([O:19][C:20]([CH3:27])([CH3:26])[C:21]([O:23][CH2:24][CH3:25])=[O:22])=[CH:17][CH:16]=3)[C:9](=[O:11])[S:10][C:6]=2[CH:5]=1)[CH3:2]

Participants

3

Reactant 2

HCID 4113O-MethylhydroxylamineHCID 22041595HCID 22041595, compound

Product 1

HCID 86760137HCID 86760137, compound

Procedure

Starting from the compound obtained in Step A, the procedure is as in Step B of Example 2, replacing the hydroxylamine by O-methylhydroxylamine. The two (Z) and (E) compounds are not separated.

Workup

  1. customThe two (Z) and (E) compounds are not separated

Sources & evidence

ORD record
ord-26fc786b3d5346d4a077959ef5fcb4b9
Source dataset
uspto-grants-2006_07
Patent number
US07071221B2

Reaction notes

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