HCID 22037985, compound → 3-Pyridineethanol

HRID 1790384Notes

Reaction equation

HRID 1790384 reaction equation
C([C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][O:11]C(C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)=[CH:5][N:4]=1)#N>C(O)=O>[N:4]1[CH:3]=[CH:8][CH:7]=[C:6]([CH2:9][CH2:10][OH:11])[CH:5]=1

Participants

3

Reactant 1

HCID 22037985HCID 22037985, compound

Product 1

HCID 805153-PyridineethanolYield 54.8%

Reagents, catalysts & solvents 1

HCID 284Formic AcidSolvent

Procedure

2-(2-Cyanopyridin-5-yl)-1-triphenylmethyloxyethane (2.631 g) and formic acid (38.0 ml) were treated as reported in Tetrahedron Lett., 579 (1986). to give the title compound (0.455 g) as colorless crystals (yield: 45.7%).

Sources & evidence

ORD record
ord-42889450e9f34e979c25d8a8947167fd
Source dataset
uspto-grants-2006_07
Patent number
US07071201B2

Reaction notes

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