HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Methoxybenzyl)triphenylphosphonium Chloride → HCID 69593617, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Methoxybenzyl)triphenylphosphonium Chloride | HCID 11407464 | — |
| Reactant | HCID 13600616 | HCID 13600616 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 69593617 | HCID 69593617 | 59.2% |
Reaction Steps
3-Methoxybenzyltriphenylphosphonium chloride (1.71 g) and 1-diethylcarbamoyl-3-formylindole (1.71 g), which had been synthesized according to the method of Tetrahedron Lett., 1869 (1986)., were reacted in tetrahydrofuran (5 ml) as in the above Production Example 41-1 to give the title compound (0.842 g) as a brown oil (yield: 59.1%). (59-2) 1-Diethylcarbamoyl-3-(3-methoxyphenethyl)indole
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07071201B2 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-64f40cb0f4e94dffa304fb3cc84114ca |
| Source note | uspto-grants-2006_07 |