Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Indoline → cis-1-(1-Acetyl-3-ethoxycarbonylpiperidin-4-yl)indoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Indoline | HCID 10328 | — |
| 반응물 | Ethyl 1-acetyl-4-oxo-3-piperidinecarboxylate | HCID 12445847 | — |
| 생성물 | cis-1-(1-Acetyl-3-ethoxycarbonylpiperidin-4-yl)indoline | HCID 59909605 | 22% |
반응 단계
Indoline (12.5 g), ethyl 1-acetyl-4-oxo-3-piperidinecarboxylate (22.3 g) and triacetoxylated sodium borohydride (48.7 g) were treated as in Example 1 to give the title compound (7.12 g) as a pale yellow powder (yield: 22%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07071201B2 |
| 출처 데이터셋 | uspto-grants-2006_07 |
| ORD ID | ord-feb2337b8d0f47378f7cf0a77a12479f |
| 출처 메모 | uspto-grants-2006_07 |