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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1790970Generated: November 2, 2026

Pyridine → HCID 7586589, compound

https://huagongshe.com/reaction/1790970

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPyridineHCID 1049—
Reactant2-MethoxyanilineHCID 7000—
Reactant2-oxo-2,3-dihydro-1H-indole-5-sulfonyl chlorideHCID 4962506—
SolventDichloromethaneHCID 6344—
ProductHCID 7586589HCID 758658937%

Reaction Steps

A solution of 5-chlorosulfonyl-2-oxindole (3 g), o-anisidine (1.8 mL) and pyridine (2.1 mL) in dichloromethane (20 mL) was stirred at room temperature for overnight at which time the red color solid was present. The solid was filtered, washed with ethanol and dried under vacuum to yield 1.5 g (37%) of 2-oxo-2,3-dihydro-1H-indole-5-sulfonic acid (2-methoxy-phenyl)-amide.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07071332B2
Source datasetuspto-grants-2006_07
ORD IDord-b71dcc59c17f45b0a42c35086404e79c
Source noteuspto-grants-2006_07