HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → N-Benzoyl-N-[3-(7-cyclopentyl-5-ethyl-4-oxo-3,4-dihydroimidazo[5,1-f][1,2,4]-triazin-2-yl)phenyl]benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 2-(3-Aminophenyl)-7-cyclopentyl-5-ethylimidazo[5,1-f][1,2,4]triazin-4(3H)-one | HCID 135682022 | — |
| Product | N-Benzoyl-N-[3-(7-cyclopentyl-5-ethyl-4-oxo-3,4-dihydroimidazo[5,1-f][1,2,4]-triazin-2-yl)phenyl]benzamide | HCID 135682042 | — |
Reaction Steps
In analogy to the procedure for Example 31, 50 mg (0.15 mmol) 2-(3-aminophenyl)-7-cyclopentyl-5-ethylimidazo[5,1-f][1,2,4]triazin-4(3H)-one (Example 29), 43 mg (0.31 mmol) benzoyl chloride and proportionate amounts of the other reagents are used.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07074790B2 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-f2177943fabb401aba978188f1d2b8c8 |
| Source note | uspto-grants-2006_07 |