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Benzenemethanamine, 3,4-dichloro- → N-(3,4-dichlorobenzyl)-N'-(3-methylcinnolin-5-yl)urea
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzenemethanamine, 3,4-dichloro- | HCID 1608 | — |
| 反応物 | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| 反応物 | 2,2,2-trichloro-N-(3-methylcinnolin-5-yl)acetamide | HCID 22032658 | — |
| 生成物 | N-(3,4-dichlorobenzyl)-N'-(3-methylcinnolin-5-yl)urea | HCID 10406258 | — |
反応手順
The title compound was prepared using 3,4-dichlorobenzylamine, the product from Example 16A, DBU and the procedure described in Example 1B. MS (ESI+) m/z 362 (M+)+; 1H NMR (DMSO-d6) δ 2.88 (s, 3H), 4.36 (d, 2H), 7.10 (t, 1H), 7.34 (dd, 1H), 7.59 (m, 2H), 7.76 (t, 1H), 8.04 (d, 2H), 8.19 (d, 1H), 8.93 (s, 1H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07074805B2 |
| 出典データセット | uspto-grants-2006_07 |
| ORD ID | ord-dd3cfb7d3b544124813d63fb69494554 |
| 出典メモ | uspto-grants-2006_07 |